Liquid-Liquid Extraction Pilot Plant vocational training equipment

LL Liquid-Liquid Extraction Pilot Plant vocational training equipment

This unit includes two separate tanks for the solvent and for the phase having to be refined, that are sent to the extraction column by two metering pumps; the column is provided with top and bottom phase separators and with two other tanks for collecting the refined and extracted products.
TRAINING PROGRAM
This unit enables to deepen the following issues:
• Determination of the number of transfer units
• Height of a transfer unit
• Extraction efficiency
• Mass balance
• Calculation of mass transfer coefficient
• Calculation of the number of theoretical stages
• Trend of concentrations along the column
• Exercises on systems of 3 partially mixable components:
- acetic acid – toluene – water
- acetic acid – isopropyl ether – water
- acetic acid – ethyl acetate – water
TECHNICAL SPECIFICATIONS:
Mod. LL

• Framework of AISI 304 stainless steel with castors
• Extraction column of borosilicate glass, DN50, consisting of 26 stages, h = 1500 mm, and including stirrer with discs of AISI 316 stainless steel , top and bottom separators of
borosilicate glass and variable speed motor (0 to 1000 rpm) with tachogenerator (for mod. LL, only)
• 4 graduated tanks of borosilicate glass, with capacity of 25 l
• Metering double-body pump of AISI 316 stainless steel, with flow rate of 0 to 30 l/h, including pneumatic actuator adjustable with signal of 0.2 to1 bar
• Pneumatic control valve of AISI 316 stainless steel, DN 15, Cv = 0.13
• Thermoresistance Pt 100 with sheath of AISI 316 stainless steel
• Electronic temperature indicator
• 3 manual pneumatic control devices
• Piping and valves of AISI 304 and 316 stainless steel
• Switchboard IP55, complying with EC conformity mark, including plant synoptic and ELCB
• Emergency button
Supply with
THEORETICAL – EXPERIMENTAL HANDBOOK